反应详情

To 1-phenyl-cyclopropanecarboxylic acid (0.500 g) in acetic acid (2 mL) was added Adams catalyst (0.050 g) in ethanol (0.3 mL). The reaction was left to stir for 48 hours under 5 bar of hydrogen. The reaction was filtered, washing with ethanol (10 mL) and water (10 mL). The resulting solid was collected by filtration and subsequently washed with water (10 mL) to afford the sub-titled compound (0.3 g).

1. waitThe reaction was left
2. filtrationThe reaction was filtered
3. washwashing with ethanol (10 mL) and water (10 mL)
4. filtrationThe resulting solid was collected by filtration
5. washsubsequently washed with water (10 mL)