HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 11277533, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Reactant | Cyclohexanemethylamine | HCID 76688 | — |
| Reactant | 5-BroMo-6-Methylquinoline | HCID 14117360 | — |
| Catalyst | HCID 178418476 | HCID 178418476 | — |
| Product | HCID 11277533 | HCID 11277533 | — |
Reaction Steps
Prepared according to the method of example 42, using 5-bromo-6-methylquinoline (prepared according to the method of Khimiya Geterotsiklicheskikh Soedinenii 1988, 8, 1084) (4.0 g), cyclohexanemethylamine (4.2 mL), triethylamine (2.4 mL), dichlorobis(triphenylphosphine)palladium(II) (1.6 g) in N-methylpyrrolidinone (40 mL) to afford the title compound (3.9 g)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07408065B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-3c435494e1504168a3b224dfb834b3d0 |
| Source note | uspto-grants-2008_08 |