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HRID2217878

反应详情

EQUATION

反应方程式

HRID 2217878 的结构方程式

REACTANTS

反应物

2
结构：NCCC1CCCCC1
HCID20509

Cyclohexaneethanamine (9CI)

C8H17N

结构：CCOC(=O)C1CCN(c2ccc3c(C(=O)O)c(Cl)ccc3n2)CC1
HCID68808948

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)C1CCN(c2ccc3c(C(=O)NCCC4CCCCC4)c(Cl)ccc3n2)CC1
HCID68808940

未命名化合物

收率 70.8%

PROCEDURE

实验过程

Prepared according to the method of example 4(a), using 6-chloro-2-[4-(ethoxycarbonyl)-1-piperidinyl]-5-quinolinecarboxylic acid (example 76(c)) (217 mg) and cyclohexaneethanamine (277 mg). Purification (SiO2, methanol:dichloromethane 1:99 as eluant) gave the title compound as a solid (200 mg).

WORKUP

后处理

  1. customPrepared
  2. customPurification (SiO2, methanol:dichloromethane 1:99 as eluant)