HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-fluoroacetoacetate → HCID 178432646, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-fluoroacetoacetate | HCID 230078 | — |
| Reactant | 1-(2-Fluorobenzyl)-1H-pyrazolo[3,4-b]pyridine-3-carboximidamide | HCID 11403986 | — |
| Product | HCID 178432646 | HCID 178432646 | — |
Reaction Steps
The compound is prepared in analogy to example I, step 6. Starting from 650 mg (2.41 mmol) of 1-(2-fluorobenzyl)-1H-pyrazolo[3,4-b]pyridine-3-carboximidamide (example I, step 5) and ethyl 2-fluoro-3-oxobutanoate, 520 mg (60% of theory) of the product are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07410973B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-555baf4f3f0f47199ce61f3482cbe0c7 |
| Source note | uspto-grants-2008_08 |