Propanolamine ethyl ether → HCID 9802227, compound

Participants

Reaction Conditions

Reaction Steps

35 mg (0.10 mmol) of 3-(4-chloro-6-methyl-2-pyrimidinyl)-1-(2-fluorobenzyl)-1H-pyrazolo[3,4-b]pyridine (example I, step 7) and 52 mg (0.50 mmol) of 3-(ethyloxy)-propylamine are dissolved in 0.40 ml of DMSO and heated at 60° C. for 48 hours. The reaction mixture is diluted with 0.20 ml of DMSO and then purified by preparative

Provenance & Evidence