HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylboronic Acid → HCID 11164299, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | 2-Chlorophenylboronic acid | HCID 2734322 | — |
| Reactant | HCID 69289305 | HCID 69289305 | — |
| Product | HCID 11164299 | HCID 11164299 | 61% |
Reaction Steps
Prepared from 5-chloro-1-methyl-7-phenyl-1,3-dihydro-benzo[e][1,4]diazepin-2-one using the same method described for Example 9 and instead of using benzene boronic acid, we used 2-chlorophenyl boronic acid. The title compound (115 mg) was obtained as a beige solid, (yield=61%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07410963B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-33c60f15a2a44bdeb385174337269031 |
| Source note | uspto-grants-2008_08 |