HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → HCID 13123247, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | 2-Fluoro-3-methoxybenzaldehyde | HCID 3774463 | — |
| Reactant | Sulfur | HCID 5362487 | — |
| Reactant | 4-Methoxybenzo[d]isothiazole | HCID 19384352 | — |
| Solvent | 2-Methoxyethanol | HCID 8019 | — |
| Product | HCID 13123247 | HCID 13123247 | 14% |
Reaction Steps
A method similar to 4-methoxy-benzo[d]isothiazole using 2-fluoro-3-methoxy-benzaldehyde (410 mg, 2.66 mmol), sulfur (85 mg, 2.66 mmol), NH4OH (5 mL), and 2-methoxyethanol (5 mL) gave the title compound (60 mg, 14%); Mass spectrum (ion-spray): m/z=165.8 (m+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07410982B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-c38e9498c7e54fdcb532a93378c659e0 |
| Source note | uspto-grants-2008_08 |