HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tributylphosphine → HCID 58612387, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tributylphosphine | HCID 13831 | — |
| Reactant | (1R)-3-chloro-1-phenylpropan-1-ol | HCID 642409 | — |
| Reactant | Thieno[3,2-b]pyridin-7-ol | HCID 5074765 | — |
| Product | HCID 58612387 | HCID 58612387 | 54% |
Reaction Steps
using (R)-(+)-3-chloro-1-phenyl-1-propanol, thieno[3,2-b]pyridin-7-ol (commercially available from the Aldrich Chemical Company), PBu3, and ADPP gave the title compound (0.71 g, 54%); Mass spectrum (ion spray): m/z=304.06 (m+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07410982B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-714621f6656c4ea1951b1aeb0f567513 |
| Source note | uspto-grants-2008_08 |