HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → 3-[4-(6-Bromo-3H-imidazo[4,5-b]pyridin-2-yl)phenoxy]propan-1-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 178514999 | HCID 178514999 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-[4-(6-Bromo-3H-imidazo[4,5-b]pyridin-2-yl)phenoxy]propan-1-amine | HCID 178511146 | — |
Reaction Steps
The title compound was prepared by stirring 2-{3-[4-(6-bromo-3H-imidazo[4,5-b]pyridin-2-yl)phenoxy]propyl}-1H-isoindole-1,3(2H)-dione with a large excess of methylamine in ethanol for two days and was purified by column chromatography on silica.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07410966B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-43569341b3ee48ef8df558257f13879a |
| Source note | uspto-grants-2008_08 |