HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 178478508, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 178521371 | HCID 178521371 | — |
| Product | HCID 178478508 | HCID 178478508 | — |
Reaction Steps
2-[4-(6-Bromo-3H-imidazo[4,5-b]pyridin-2-yl)phenoxy]ethanol (2.0 g, 6 mmol) was dissolved and refluxed in thionyl chloride (30 ml) for 3 h. The excess thionyl chloride was evaporated off and the residue was co-evaporated twice with toluene affording the title product in quantitative yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07410966B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-bd7866aa653949939d6bd8c419b26d6d |
| Source note | uspto-grants-2008_08 |