HuagongsheHuagongshe Chemistry Print Report · For research reference only
Malononitrile → HCID 178423906, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Malononitrile | HCID 8010 | — |
| Reactant | HCID 86600556 | HCID 86600556 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178423906 | HCID 178423906 | — |
Reaction Steps
A mixture of 1.2 g (2.82 mmol) of 11, 190 mg (2.87 mmol) of malononitrile and 0.4 ml (2.85 mmol) of TEA in 15 ml of ethanol was stirred at room temperature for 2.5 h. Then solvent was removed by a rotary evaporator. Product 12 was used in next synthesis without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07411068B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-0ce75da7a76c4ad3ade620c5e25afcc5 |
| Source note | uspto-grants-2008_08 |