HCID 66775446, compound → HCID 58807411, compound

HRID 2218572Notes

Reaction equation

HRID 2218572 reaction equation
[Br:1][C:2]1[CH:3]=[C:4]([F:15])[C:5]([CH:9]=[CH:10][C@H:11]([CH3:14])[CH2:12][CH3:13])=[C:6]([F:8])[CH:7]=1>CCCCCCC.[Pt]>[Br:1][C:2]1[CH:7]=[C:6]([F:8])[C:5]([CH2:9][CH2:10][C@H:11]([CH3:14])[CH2:12][CH3:13])=[C:4]([F:15])[CH:3]=1

Participants

4

Reactant 1

HCID 66775446HCID 66775446, compound

Product 1

HCID 58807411HCID 58807411, compound

Reagents, catalysts & solvents 2

HCID 23939PlatinumCatalystHCID 8900HeptaneSolvent

Procedure

0.4 g of 5% Pt/C (dry) is added to a solution of 1.8 g (5.9 mmol) of 2 in 50 ml of heptane, and the mixture is hydrogenated at atmospheric pressure for 20 hours. The solvent is removed under reduced pressure, and the entire amount is converted into 4.

Workup

  1. customThe solvent is removed under reduced pressure

Sources & evidence

ORD record
ord-46012c20475548efb93d71489ba5700c
Source dataset
uspto-grants-2008_08
Patent number
US07411100B2

Reaction notes

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