1-Propanesulfonyl chloride → HCID 59770420, compound

Participants

Reaction Steps

Following procedures essentially as described in Example 90, 3-(10,11-dihydro-dibenzo[a,d]cyclohepten-5-ylidenemethyl)-phenylamine (50 mg, 0.168 mmol) and 1-propanesulfonyl chloride (144 mg, 1.01 mmol) affords 34 mg (50%) of the title compound as a white foam. MS (ES) 426 M+Na), 402 (M−H); HPLC shows 99% purity.

Provenance & Evidence