HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butanesulfonyl chloride → HCID 59770388, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butanesulfonyl chloride | HCID 75430 | — |
| Reactant | HCID 59769897 | HCID 59769897 | — |
| Product | HCID 59770388 | HCID 59770388 | 58.4% |
Reaction Steps
Following procedures essentially as described in Example 90, 3-(10,11-dihydro-dibenzo[a,d]cyclohepten-5-ylidenemethyl)-phenylamine (50 mg, 0.168 mmol) and 1-butanesulfonyl chloride (158 mg, 1.01 mmol) affords 41 mg (58%) of the title compound as a colorless oil. MS (ES) 440 (M+Na); HPLC shows 99% purity.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07411072B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-11c1f52eba174d849177e58a1fe94da5 |
| Source note | uspto-grants-2008_08 |