HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Propanesulfonyl chloride → HCID 59770266, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Propanesulfonyl chloride | HCID 66279 | — |
| Reactant | HCID 59769900 | HCID 59769900 | — |
| Product | HCID 59770266 | HCID 59770266 | 51% |
Reaction Steps
Following procedures essentially as described in Example 90, 4-(10,11-dihydro-dibenzo[a,d]cyclohepten-5-ylidenemethyl)-phenylamine (100 mg, 0.336 mmol) and 1-propanesulfonyl chloride (144 mg, 1.01 mmol) affords 69 mg (51%) of the title compound as a colorless oil. MS (ES) 426 (M+Na), 402 (M−H); HPLC shows 99% purity.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07411072B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-c84bb09825034934be573a23c7d76b68 |
| Source note | uspto-grants-2008_08 |