HuagongsheHuagongshe Chemistry Print Report · For research reference only
10,11-dihydro-5H-dibenzo(a,d)cycloheptene → HCID 59769864, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 10,11-dihydro-5H-dibenzo(a,d)cycloheptene | HCID 70029 | — |
| Reactant | 2-Fluoro-5-methoxybenzaldehyde | HCID 2734872 | — |
| Product | HCID 59769864 | HCID 59769864 | 6.4% |
Reaction Steps
Following procedures essentially as described in Example 28 and using 2-fluoro-5-methoxybenzaldehyde (1.59 g, 10.3 mmol) and dibenzosuberane (1.94 g, 10 mmol), provides 210 mg of title compound as white crystals. mp 110.7° C. (hexane). HPLC shows 99% purity.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07411072B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-4496c38afd0148d7a2943a050cb1fde9 |
| Source note | uspto-grants-2008_08 |