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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2218677Generated: October 31, 2026

10,11-dihydro-5H-dibenzo(a,d)cycloheptene → HCID 59770425, compound

https://huagongshe.com/reaction/2218677

Reaction equation

Participants

RoleNameHCIDCharge
Reactant10,11-dihydro-5H-dibenzo(a,d)cyclohepteneHCID 70029—
Reactant2-Fluoro-3-methoxybenzaldehydeHCID 3774463—
ProductHCID 59770425HCID 5977042529.5%

Reaction Steps

Following procedures essentially as described in Example 28 and using 2-fluoro-3-methoxybenzaldehyde (2.4 g, 15.4 mmol) and dibenzosuberane (3.0 g, 15.4 mmol), provides 1.5 g of title compound as white crystals. mp 148.9° C. HPLC shows 96% purity.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07411072B2
Source datasetuspto-grants-2008_08
ORD IDord-cf71ab69cd8a4684a42143b18755c728
Source noteuspto-grants-2008_08