HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Trifluoromethyl)phenylboronic acid → HCID 68937781, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Trifluoromethyl)phenylboronic acid | HCID 2734389 | — |
| Reactant | 5-bromomethylene-2-chloro-10,11-dihydro-5H-dibenzo[a,d]cycloheptene | HCID 68886819 | — |
| Product | HCID 68937781 | HCID 68937781 | — |
Reaction Steps
Following procedures essentially as described in Example 219, below, and using 4-(trifluoromethyl)phenylboronic acid (114 mg, 0.60 mmol) and 5-bromomethylene-2-chloro-10,11-dihydro-5H-dibenzo[a,d]cycloheptene (156 mg, 0.48 mmol) provides the title compound. GC/MS data: retention times in minutes (MS data for M+.ion): 18.52 (384), 18.78(384)Mass Spec (EI+) 384.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07411072B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-f68440935eff4408a036fed409533ff6 |
| Source note | uspto-grants-2008_08 |