Hydrochloric Acid → HCID 68974653, compound

Participants

Reaction Steps

In an analogous procedure to that described in Example 1d), the treatment of the [(S)-4-oxo-1-(4,4,4-trifluoro-butyl)-2,3,4,5-tetrahydro-1H-benzo[b][1,4]diazepin-3-yl]-carbamic acid tert-butyl ester with hydrochlorid acid (37%) in dioxane yielded the title compound as a light yellow solid; MS (m/e): 288 (M+H)+.

Provenance & Evidence