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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2219022Generated: November 1, 2026

Hydrochloric Acid → HCID 25242115, compound

https://huagongshe.com/reaction/2219022

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 59718700HCID 59718700—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 25242115HCID 25242115—

Reaction Steps

In an analogous manner to that described in Example 1d), the treatment of the [(S)-1-(2-benzyloxy-ethyl)-4-oxo-2,3,4,5-tetrahydro-1H-benzo[b][1,4]diazepin-3-yl]-carbamic acid tert-butyl ester with hydrochlorid acid (37%) in dioxane yielded the title compound as a light yellow foam; MS (m/e): 312 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07414049B2
Source datasetuspto-grants-2008_08
ORD IDord-c3c9f1e2151a4793af1473b0b01b100d
Source noteuspto-grants-2008_08