HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 25242115, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 59718700 | HCID 59718700 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 25242115 | HCID 25242115 | — |
Reaction Steps
In an analogous manner to that described in Example 1d), the treatment of the [(S)-1-(2-benzyloxy-ethyl)-4-oxo-2,3,4,5-tetrahydro-1H-benzo[b][1,4]diazepin-3-yl]-carbamic acid tert-butyl ester with hydrochlorid acid (37%) in dioxane yielded the title compound as a light yellow foam; MS (m/e): 312 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07414049B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-c3c9f1e2151a4793af1473b0b01b100d |
| Source note | uspto-grants-2008_08 |