Water → HCID 58816127, compound

Participants

Reaction Steps

A stirred mixture of isoquinoline-5-sulfonic acid {2-[2-(4-bromo-phenylsulfanyl)-ethylamino]-ethyl}-amide (73.0 mg, 0.157 mmol) and oxone (289 mg, 0.470 mmol) in CH3OH (5 mL)/H2O (1.3 mL) is allowed to stir at ambient temperature for 30 minutes to form a suspension. After filtration, the white solid is sonicated in H2O (10 mL), then filtered to give a tan solid of the title compound. ESIMS: m/z 498 [(M+H)+, 79Br], 500 [(M+H)+, 81Br].

Provenance & Evidence