HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloroaniline → HCID 68880662, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloroaniline | HCID 7812 | — |
| Reactant | 5-(chloromethyl)-1-methyl-1H-1,2,3,4-tetrazole | HCID 12205086 | — |
| Product | HCID 68880662 | HCID 68880662 | 36.3% |
Reaction Steps
The same procedure as step 2 of example 1 was accomplished except for using p-chloroaniline (5.8 g, 45.3 mmol) and 5-chloromethyl-1-methyl-1H-tetrazol (6 g, 45.3 mmol). The crude product was purified by silica gel column chromatography (developing solvent-n-hexane:ethyl acetate=2:1), to give desired compound (3.68 g, yield: 36%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07414068B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-e1b51ef173634852817c3cb3d00faa62 |
| Source note | uspto-grants-2008_08 |