HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11097971, compound → HCID 69216536, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11097971 | HCID 11097971 | — |
| Reactant | HCID 45095277 | HCID 45095277 | — |
| Product | HCID 69216536 | HCID 69216536 | 22% |
Reaction Steps
The same procedure as step 3 of example 1 was accomplished, except for using the epoxide compound (270 mg, 0.98 mmol) obtained in step 1 of example 2 and N-(2-ethylphenyl)-N-(2-methyl-2H-tetrazol-5-ylmethyl)amine. The crude product was purified by silica gel column chromatography (developing solvent-n-hexane:ethyl acetate=1:2), to give desired compound (100 mg, yield: 22%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07414068B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-eb3acc1750f8465ea4d1a59e16700a29 |
| Source note | uspto-grants-2008_08 |