HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Methylthio)phenylboronic acid → HCID 67421064, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Methylthio)phenylboronic acid | HCID 2733959 | — |
| Reactant | HCID 178434980 | HCID 178434980 | — |
| Product | HCID 67421064 | HCID 67421064 | 45% |
Reaction Steps
As described for Example 3, 4-(1H-imidazol-4-yl)-5-methyl-3-phenyl-isoxazole (112.6 mg, 0.5 mmol) was converted, using 4-methylthiophenylboronic acid instead of 4-fluorophenylboronic acid, to the title compound (78 mg, 45%) which was obtained as a white solid. MS (ESI): m/e=348.0 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07414061B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-c9ce726aa28b49889b18b8ea579b25b4 |
| Source note | uspto-grants-2008_08 |