HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Fluoronitrobenzene → HCID 23725438, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Fluoronitrobenzene | HCID 9590 | — |
| Reactant | HCID 178434974 | HCID 178434974 | — |
| Product | HCID 23725438 | HCID 23725438 | 39% |
Reaction Steps
As described for Example 44, 3-(3-bromo-phenyl)-4-(1H-imidazol-4-yl)-5-methyl-isoxazole (91 mg, 0.3 mmol) using 1-fluoro-4-nitrobenzene instead of 4-fluoroacetophenone was converted to the title compound (50 mg, 39%) which was obtained as a light yellow solid. MS: m/e=425.1/427.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07414061B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-3d82fe38e32c4632822aada8acd13338 |
| Source note | uspto-grants-2008_08 |