HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Fluoronitrobenzene → HCID 23725484, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Fluoronitrobenzene | HCID 9590 | — |
| Reactant | HCID 178432460 | HCID 178432460 | — |
| Product | HCID 23725484 | HCID 23725484 | 36% |
Reaction Steps
As described for Example 57, 5-methyl-4-(2-methyl-1H-imidazol-4-yl)-3-phenyl-isoxazole (70 mg, 0.3 mmol) using 1-fluoro-4-nitrobenzene instead of 4-fluoroacetophenone was converted to the title compound (38 mg, 36%) which was obtained as an off-white solid. MS: m/e=361.4 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07414061B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-f862f3b9de514e99be8631c3bd1d9277 |
| Source note | uspto-grants-2008_08 |