HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-methoxyacetoacetate → HCID 67420638, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-methoxyacetoacetate | HCID 123500 | — |
| Reactant | Alpha-chlorobenzaldoxime | HCID 5706359 | — |
| Product | HCID 67420638 | HCID 67420638 | — |
Reaction Steps
As described for Example 36c, (E)- and/or (Z)-N-hydroxy-benzenecarboximidoyl chloride (14.04 g, 90 mmol) was converted, using 4-methoxy-3-oxo-butyric acid methyl ester instead of acteylacetone to the crude title compound (18.76 g) which was obtained as an off-white solid and used directly in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07414061B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-17851a5b2f5a44b1a06242f6a64200cd |
| Source note | uspto-grants-2008_08 |