Bromobenzene → HCID 69351716, compound

HRID 2219517Notes

Reaction equation

HRID 2219517 reaction equation
[CH3:1][N:2]1[CH:6]=[CH:5][C:4]([NH:7][C:8]([C:10]2[C:15]([NH:16][C:17]3[CH:18]=N[CH:20]=[CH:21][CH:22]=3)=[CH:14][CH:13]=[C:12]([CH3:23])[N:11]=2)=[O:9])=[N:3]1.Br[C:25]1C=CC=CC=1>>[CH3:1][N:2]1[CH:6]=[CH:5][C:4]([NH:7][C:8]([C:10]2[C:15]([NH:16][C:17]3[CH:22]=[CH:21][CH:20]=[CH:25][CH:18]=3)=[CH:14][CH:13]=[C:12]([CH3:23])[N:11]=2)=[O:9])=[N:3]1

Participants

3

Reactant 2

HCID 7961BromobenzeneHCID 11573128HCID 11573128, compound

Product 1

HCID 69351716HCID 69351716, compound

Procedure

The title compound, was prepared from 3-Amino-6-methyl-pyridine-2-carboxylic acid (1-methyl-1H-pyrazol-3-yl)-amide (example 16) in accordance with the general method of example 20 using Bromobenzene instead of 3-Bromo-4-methylpyridine to yield the final compound as a yellow solid, MS (ISP): m/e=308.4 (M+H+).

Sources & evidence

ORD record
ord-6ac52fdbf8fd4e0ebb1d26439c1f6ca3
Source dataset
uspto-grants-2008_08
Patent number
US07414060B2

Reaction notes

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