HRID2219670

反应详情

EQUATION

反应方程式

HRID 2219670 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a suspension of 0.25 g (1.6 mmol) of N-cyclohexylthiourea in 2.5 mL of ethanol was added 0.31 g of ethyl bromopyruvate. The reaction was heated at reflux for 17 hr then evaporated to leave the title compound.

WORKUP

后处理

  1. temperatureThe reaction was heated
  2. temperatureat reflux for 17 hr
  3. customthen evaporated