HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyamine hydrochloride → 5-[(1E)-1-hydroxyimino-3-methyl-2,3-dihydroinden-5-yl]-1-methylpyrrole-2-carbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | 1-methyl-5-(3-methyl-1-oxo-2,3-dihydro-1H-inden-5-yl)-1H-pyrrole-2-carbonitrile | HCID 24986668 | — |
| Product | 5-[(1E)-1-hydroxyimino-3-methyl-2,3-dihydroinden-5-yl]-1-methylpyrrole-2-carbonitrile | HCID 16226365 | — |
Reaction Steps
The title compound was prepared from 1-methyl-5-(3-methyl-1-oxo-2,3-dihydro-1H-inden-5-yl)-1H-pyrrole-2-carbonitrile and hydroxylamine hydrochloride according to the procedure described in example 1. MS m/z 266; HRMS: calcd for C16H15N3O+H+, 266.12879; found (ESI, [M+H]+), 266.1299; Anal. Calcd for C16H15N3O: C, 72.43; H, 5.70; N, 15.84. Found: C, 71.86; H, 6.31; N, 15.47.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07414142B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-516ad9cca6e94f099fa95421c1b20ba9 |
| Source note | uspto-grants-2008_08 |