HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Cyclohexen-1-one, 4,4-dimethyl- → Cyclohexanone, 4,4-dimethyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Cyclohexen-1-one, 4,4-dimethyl- | HCID 136839 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | Cyclohexanone, 4,4-dimethyl- | HCID 138166 | — |
Reaction Steps
0.5 g 10% palladium on charcoal are added to a solution of 5.00 g 4,4-dimethyl-cyclohex-2-enone in 25 ml of ethyl acetate. The mixture is shaken under a hydrogen pressure of 25 psi for 3 h at ambient temperature. Then the catalyst is filtered off and the solvent is removed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07417032B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-e9005a3403424f46a673180156dda472 |
| Source note | uspto-grants-2008_08 |