HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 58229873, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | HCID 58229897 | HCID 58229897 | — |
| Product | HCID 58229873 | HCID 58229873 | — |
Reaction Steps
A mixture of 3-chloro-9-(chloromethyl)-2-phenyl[1,2,4]triazolo[4′,3′:1,6]pyrido[2,3-b]pyrazine (10-2) (840 mg, 0.254 mmol) and dimethylamine (2M in THF, 5 mL, 10 mmol) was stirred at room temperature for 2 hours. The solvent was evaporated to give 1-(3-chloro-2-phenyl[1,2,4]triazolo[4′,3′:1,6]pyrido[2,3-b]pyrazin-9-yl)-N,N-dimethylmethanamine (10-3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08207169B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-f380907a062742d39276524a0d263255 |
| Source note | uspto-grants-2012_06 |