HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxy-alpha-toluenethiol → Ethyl 6-[(4-methoxybenzyl)sulfanyl]-1-cyclohexene-1-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxy-alpha-toluenethiol | HCID 80407 | — |
| Reactant | ethyl 6-[N-(2,4-difluorophenyl)sulfamoyl]-1-cyclohexene-1-carboxylate | HCID 9928140 | — |
| Product | Ethyl 6-[(4-methoxybenzyl)sulfanyl]-1-cyclohexene-1-carboxylate | HCID 22026134 | 95.6% |
Reaction Steps
In the same manner as in Reference Example 1, ethyl 6-[N-(2,4-difluorophenyl)sulfamoyl]-1-cyclohexene-1-carboxylate (1 g) and (4-methoxyphenyl)methanethiol (893 mg) were reacted to give ethyl 6-[(4-methoxybenzyl)-sulfanyl]-1-cyclohexene-1-carboxylate (848 mg) as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07417059B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-2059ab0cc1d9426ea6c079d8eaa7392c |
| Source note | uspto-grants-2008_08 |