HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → (2-Bromo-benzyl)-diethyl-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | 2-Bromobenzyl bromide | HCID 76965 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | (2-Bromo-benzyl)-diethyl-amine | HCID 10083076 | — |
Reaction Steps
To 1-Bromo-2-bromomethyl-benzene (2.17 g, 0.008 mmol) in toluene (15 mL) was added diethylamine (3.05 mL) and the mixture was stirred at room temperature for 14 hours. The reaction mixture was filtered and concentrated to give Example 229A as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07417040B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-ca758fde160a49c097dfedcef981117c |
| Source note | uspto-grants-2008_08 |