HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → 2-Bromobenzohydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | Methyl 2-bromobenzoate | HCID 11894 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-Bromobenzohydrazide | HCID 101460 | — |
Reaction Steps
A solution of methyl 2-bromobenzoate (1.0 g, 4.7 mmol) in EtOH (15 mL) was treated with hydrazine (0.18 mL, 5.6 mmol) and heated to reflux for 15 hours. The resulting solution was concentrated to a white powder (998 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07417040B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-06912a1921b247f1b6541797231ef7e6 |
| Source note | uspto-grants-2008_08 |