HCID 68968184, compound → HCID 11660395, compound

Participants

Reaction Steps

To a solution of compound Example 287B (8 mg, 0.023 mmol) in MeOH (5 mL) was added Pd(OH)2/C (26 mg). The mixture was stirred at room temperature under a hydrogen atmosphere for 2 hours. The solution was filtered through a nylon membrane filter, concentrated and purified by preparative HPLC to give the title compound (3 mg, 37%). HPLC Rt=3.517 min. m/z=356(M+H+).

Provenance & Evidence