HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 11989687, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 11989686 | HCID 11989686 | — |
| Solvent | Water ethanol | HCID 19096565 | — |
| Product | HCID 11989687 | HCID 11989687 | — |
Reaction Steps
According to Step 5, after reaction of 5-(4-tert-Butylbenzenesulfonylamino)-3-phenyl-1-benzothiophene-2-carboxylic acid ethyl ester (1.24 g, 2.5 mmol) from Example 1d) with 1M sodium hydroxide solution in ethanol/water (2:1, 49 mL), the desired compound is obtained at quantitative yield (1.18 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07417066B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-4f2ea0e2651d4ea4a2297ff55341a28f |
| Source note | uspto-grants-2008_08 |