HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methylpiperazine → HCID 67311978, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Reactant | HCID 58346788 | HCID 58346788 | — |
| Product | HCID 67311978 | HCID 67311978 | 100% |
Reaction Steps
This compound was prepared in a similar fashion as described in Example 48 step 6 starting from 3-(2-bromo-ethyl)-6-[2-(4-nitro-phenyl)-ethoxy]-4,5-dihydro-3H-10-thia-2,3,7,9-tetraaza-cyclopenta[a]fluorene (2.6 g, 5.2 mmol) and N-methyl piperazine (1.56 g, 15.59 mmol). The crude desired product was obtained as a light yellow solid (2.7 g) in 100% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08207172B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-46e3d3f5b94c4aebb56155f831cec944 |
| Source note | uspto-grants-2012_06 |