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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 222058Generated: November 2, 2026

1-Methylpiperazine → HCID 67311978, compound

https://huagongshe.com/reaction/222058

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-MethylpiperazineHCID 53167—
ReactantHCID 58346788HCID 58346788—
ProductHCID 67311978HCID 67311978100%

Reaction Steps

This compound was prepared in a similar fashion as described in Example 48 step 6 starting from 3-(2-bromo-ethyl)-6-[2-(4-nitro-phenyl)-ethoxy]-4,5-dihydro-3H-10-thia-2,3,7,9-tetraaza-cyclopenta[a]fluorene (2.6 g, 5.2 mmol) and N-methyl piperazine (1.56 g, 15.59 mmol). The crude desired product was obtained as a light yellow solid (2.7 g) in 100% yield.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08207172B2
Source datasetuspto-grants-2012_06
ORD IDord-46e3d3f5b94c4aebb56155f831cec944
Source noteuspto-grants-2012_06