HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23655921, compound → HCID 23655159, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23655921 | HCID 23655921 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 23655159 | HCID 23655159 | — |
Reaction Steps
Following the procedure described above for 95, 101 was prepared from 94 to 100 as a white solid (0.6 g, 24%): mp 175-177° C. (CH2Cl2). 1H NMR (DMSO-d6) δ8.04 (b, 2H), 7.83 (dd, J=8.2, 1.1 Hz, 2H), 7.65 (d, J=8.2 Hz, 2H), 6.83 (s, 2H), 3.87 (s, 6H), 3.33 (s, 4H). HPLC (method B) tR 9.16 min (100.00 area %). Anal. (C22H18O6) C, H.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07417158B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-b32510fade6e4262b20879edd33d2428 |
| Source note | uspto-grants-2008_08 |