HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Naphthaldehyde → HCID 59772995, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Naphthaldehyde | HCID 6195 | — |
| Reactant | 2-(2-Aminoethyl)-1-methylpyrrolidine | HCID 98388 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 59772995 | HCID 59772995 | — |
Reaction Steps
Experimental condition analogous to Example 5, from 1-naphthalencarboxaldehyde 0.15 g (1 mmol), 2-(1-methyl-pyrrolidin-2-yl)-ethylamine 0.14 g (1.1 mmol), and sodium triacethoxyborohydride 0.31 g (1.5 mmol), in 10 mL dichloromethane. The crude material is 210 mg clear oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07417062B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-f1bd77258f484cd889301f69ec669b22 |
| Source note | uspto-grants-2008_08 |