HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-Aminoethyl)-1-methylpyrrolidine → HCID 59502240, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-Aminoethyl)-1-methylpyrrolidine | HCID 98388 | — |
| Reactant | 1-methyl-1H-1,3-benzodiazole-2-carbaldehyde | HCID 762084 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 59502240 | HCID 59502240 | — |
Reaction Steps
Experimental condition analogous to Example 5, from 1-methyl-1H-benzoimidazol-2-carbaldehyde 0.2 g (1.25 mmol), 2-(1-methyl-pyrrolidin-2-yl)-ethylamine 0.18 g (1.38 mmol), and sodium triacethoxyborohydride 0.39 g (1.87 mmol), in 10 mL dichloromethane. After work-up the material was used as a crude.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07417062B2 |
| Source dataset | uspto-grants-2008_08 |
| ORD ID | ord-1a58457db96345a8b58907a9d21d492b |
| Source note | uspto-grants-2008_08 |