HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butoxycarbonyl-D-leucine → HCID 59709937, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butoxycarbonyl-D-leucine | HCID 637604 | — |
| Reactant | HCID 68801862 | HCID 68801862 | — |
| Product | HCID 59709937 | HCID 59709937 | — |
Reaction Steps
N-(tert-Butoxycarbonyl)-D-leucine (540 mg, 2.32 mmol) and benzyl 3-cyclopropyl-L-alaninate hydrochloride (Example 3A, 490 mg, 1.93 mmol) are reacted by general procedure 6. The crude product is purified by preparative HPLC, (method 16), resulting in a quantitive yield of the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07368424B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-2babaaee8faa4a2e924b9afd581c7aec |
| Source note | uspto-grants-2008_05 |