HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbodiimide → HCID 60208253, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbodiimide | HCID 160435 | — |
| Reactant | HCID 60208254 | HCID 60208254 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 60208253 | HCID 60208253 | — |
Reaction Steps
N-(3-{2-[2-fluoro-4-(methyloxy)phenyl]ethyl}-4-oxo-3,4-dihydro-7-quinazolinyl)-N′-[(1S,2S,3S,5R)-2,6,6-trimethylbicyclo[3.1.1]hept-3-yl]thiourea was gently stirred with Argonaut PS-Carbodiimide (1.5 eq) for 15 hours in THF. The resin was filtered off and the solution of carbodiimide A was diluted to a known volume to give a solution of known molarity.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07368453B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-d28bc2157cd14a008b56cfd5000ad163 |
| Source note | uspto-grants-2008_05 |