HCID 23089328, compound → HCID 86605945, compound

Participants

Reaction Steps

100 ml of dichloromethane and 28.61 g of sodium 2-(bicyclo[2.2.1]heptan-2-yl)tetrafluoroethane sulfonate were added to the aqueous solution of 1-(6-n-butoxynaphthalen-2-yl)tetrahydrothiophenium methane sulfonate and the mixture was stirred for 12 hours. After removing the water layer using a separating funnel, the organic layer was washed five times with 40 ml of purified water. The solvent was evaporated using a rotary evaporator under reduced pressure by a stream aspirator at room temperature and the residue was dried at 50° C. under reduced pressure to obtain 24.2 g of 1-(6-n-butoxynaphthalen-2-yl)tetrahydrothiophenium 2-(bicyclo[2.2.1]heptan-2-yl)tetrafluoroethane sulfonate as a white solid.

Provenance & Evidence