HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromotrimethylsilane → HCID 22349213, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromotrimethylsilane | HCID 76113 | — |
| Reactant | 2,4-Dichloro-5-(diethylphosphonomethoxymethyl)thiazole | HCID 57457791 | — |
| Product | HCID 22349213 | HCID 22349213 | — |
Reaction Steps
2,4-Dichloro-5-(diethylphosphonomethoxymethyl)thiazole was deesterified with TMSBr as described in Step D, Example 1, to provide the title compound (no. 14.01) as a solid. HPLC Rt=4.36 min; negative ion electrospray MS M-1 found: 276/278.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07371739B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-870050b383504dd190f27bcb7e63cbc2 |
| Source note | uspto-grants-2008_05 |