HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2222128Generated: October 31, 2026
HCID 86603475, compound → HCID 11712998, compound
https://huagongshe.com/reaction/2222128
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 86603475 | HCID 86603475 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 11712998 | HCID 11712998 | — |
Reaction Steps
33 mg (0.045 mmol) benzyl (3-{4-[4-((R)-7-ethyl-8-isopropyl-5-methyl-6-oxo-5,6,7,8-tetrahydro-pteridin-2-ylamino)-3-methoxy-phenyl]-piperazin-1-yl}-propyl)-carbamate are taken up in 5 ml of methanol combined with 4 mg palladium hydroxide and stirred for 24 h at 20° C. and 7 bar hydrogen pressure. Then the catalyst is filtered off and the solvent is eliminated in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07371753B2 |
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| Source dataset | uspto-grants-2008_05 |
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| ORD ID | ord-117ebf5dde2f4cfd8580ccaefe2cde7d |
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| Source note | uspto-grants-2008_05 |
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