HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl chloroformate → HCID 11774849, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl chloroformate | HCID 15891 | — |
| Reactant | 1,4-Dioxa-8-azaspiro(4.5)decane | HCID 67435 | — |
| Reactant | 4-Methoxy-7-(tetrahydro-pyran-4-yl)-benzothiazol-2-yl-amine | HCID 22015735 | — |
| Product | HCID 11774849 | HCID 11774849 | — |
Reaction Steps
Using 4-methoxy-7-(tetrahydro-pyran-4-yl)-benzothiazol-2-ylamine, phenyl chloroformate and 1,4-dioxa-8-aza-spiro[4.5]decane, the title compound was prepared as white crystals (53% yield). MS: m/e=434(M+H+), mp 208-209° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07371748B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-fe92be28f6fa48bbadd6f308df006e56 |
| Source note | uspto-grants-2008_05 |