HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluoro-3-methylbenzoic acid → N-(7-[1,4]Dioxepan-6-yl-4-methoxy-benzothiazol-2-yl)-4-fluoro-3-methyl-benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluoro-3-methylbenzoic acid | HCID 242828 | — |
| Reactant | 5-Methyl-thiophene-2-carboxylic acid (7-[1,4]dioxepan-6-yl-4-methoxy-benzothiazol-2-yl)-amide | HCID 11373100 | — |
| Reactant | 7-[1,4]Dioxepan-6-yl-4-methoxy-benzothiazol-2-ylamine | HCID 59711805 | — |
| Product | N-(7-[1,4]Dioxepan-6-yl-4-methoxy-benzothiazol-2-yl)-4-fluoro-3-methyl-benzamide | HCID 86595144 | — |
Reaction Steps
Using 7-[1,4]dioxepan-6-yl-4-methoxy-benzothiazol-2-ylamine and 4-fluoro-3-methyl-benzoic acid, the title compound was prepared in the same manner as described for 5-methyl-thiophene-2-carboxylic acid (7-[1,4]dioxepan-6-yl-4-methoxy-benzothiazol-2-yl)-amide and obtained as light brown powder. MS: m/e=417(M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07371748B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-2e4f2becd4ee476391487e3db8788fff |
| Source note | uspto-grants-2008_05 |