Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(2-Methoxyethyl)(methyl)amine → HCID 86595148, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (2-Methoxyethyl)(methyl)amine | HCID 300977 | — |
| 반응물 | 2-(2-Methoxy-ethylamino)-N-(4-methoxy-7-morpholin-4-yl-benzothiazol-2-yl)-isonicotinamide | HCID 10288248 | — |
| 반응물 | HCID 86595149 | HCID 86595149 | — |
| 생성물 | HCID 86595148 | HCID 86595148 | — |
반응 단계
N-(7-[1,4]Dioxepan-6-yl-4-methoxy-benzothiazol-2-yl)-bromo-isonicotinamide and N-(2-methoxyethyl)-methylamine were reacted as described for 2-(2-methoxy-ethylamino)-N-(4-methoxy-7-morpholin-4-yl-benzothiazol-2-yl)-isonicotinamide in WO03/043636. Usual workup, preparative reversed-phase HPLC and final dry-freezing afforded the title compound as light brown solid. MS: m/e=473(M+H+).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07371748B2 |
| 출처 데이터셋 | uspto-grants-2008_05 |
| ORD ID | ord-27116f15c29c42a5ac142b9986c83aff |
| 출처 메모 | uspto-grants-2008_05 |