HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Oxolan-2-yl)acetic acid → HCID 86595154, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Oxolan-2-yl)acetic acid | HCID 228726 | — |
| Reactant | HCID 11257802 | HCID 11257802 | — |
| Reactant | 4-Methoxy-7-(tetrahydro-pyran-4-yl)-benzothiazol-2-yl-amine | HCID 22015735 | — |
| Product | HCID 86595154 | HCID 86595154 | — |
Reaction Steps
Using 4-methoxy-7-(tetrahydro-pyran-4-yl)-benzothiazol-2-ylamine and (tetrahydro-furan-2-yl)-acetic acid, the title compound was prepared in the same manner as described for N-[4-methoxy-7-(tetrahydro-pyran-4-yl)-benzothiazol-2-yl]-2-(tetrahydro-pyran-4-yl)-acetamide and obtained as white solid (50% yield). Mp 170-174° C., MS: m/e=377(M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07371748B2 |
| Source dataset | uspto-grants-2008_05 |
| ORD ID | ord-e09fdb9649a742eb815a3702b02fb18d |
| Source note | uspto-grants-2008_05 |